Investigating the effects of laser wavelengths and other ablation parameters on the detection of biogenic elements and contaminants in hydroxyapatite

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dc.contributor.authorFazlić, Aidacs
dc.contributor.authorFaruzelová, Annacs
dc.contributor.authorBuday, Jakubcs
dc.contributor.authorMichlovská, Lenkacs
dc.contributor.authorVojtová, Lucycs
dc.contributor.authorModlitbová, Pavlínacs
dc.contributor.authorPořízka, Pavelcs
dc.contributor.authorKaiser, Jozefcs
dc.coverage.issue9cs
dc.coverage.volume39cs
dc.date.accessioned2024-12-10T13:55:41Z
dc.date.available2024-12-10T13:55:41Z
dc.date.issued2024-08-28cs
dc.description.abstractThe main purpose of this work is to thoroughly describe sensitivity and resolution enhancement by systematically optimizing key parameters in laser-induced breakdown spectroscopy analysis. Simultaneous analysis of biogenic (C, P, Mg, and Ca) and contaminating (Pb) elements, which are commonly detected in selected biotic matrices (mammal teeth), was performed. Hydroxyapatite reference pellets were utilized as model matrices, which successfully reflect human dental tissue. The optimization involved precise adjustments of the used laser wavelengths (1064, 532, and 266 nm), relative defocus of the laser pulse, ablation pulse energies, and gate delays for collecting characteristic spectra. In addition, for Ca analysis, the signals of different ionization line types (Ca I 364.44 nm; Ca II 370.60 and 396.85 nm) were compared; in the case of Pb analysis, the limits of detection were established for each used laser wavelength, and the revealed differences were discussed in detail. We intend to demonstrate the benefits of rapid, low-cost analysis and also the importance of measurement parameters used in biotic sample testing. A comparison of laser ablation measurement parameters (laser wavelength, energy, gate delay, defocus, and spot size) to determine optimal settings for the detection of heavy metals and biogenic elements in a hard tissue matrix (hydroxyapatite).en
dc.formattextcs
dc.format.extent2330-2339cs
dc.format.mimetypeapplication/pdfcs
dc.identifier.citationJournal of Analalytical Atomic Spectrometry. 2024, vol. 39, issue 9, p. 2330-2339.en
dc.identifier.doi10.1039/d4ja00073kcs
dc.identifier.issn0267-9477cs
dc.identifier.orcid0009-0006-4285-2916cs
dc.identifier.orcid0000-0001-8296-3828cs
dc.identifier.orcid0000-0003-1453-5068cs
dc.identifier.orcid0000-0002-7963-1715cs
dc.identifier.orcid0000-0001-5281-7045cs
dc.identifier.orcid0000-0003-4970-356Xcs
dc.identifier.orcid0000-0002-8604-7365cs
dc.identifier.orcid0000-0002-7397-125Xcs
dc.identifier.other189905cs
dc.identifier.researcheridKCZ-1616-2024cs
dc.identifier.researcheridKIE-3874-2024cs
dc.identifier.researcheridB-1133-2014cs
dc.identifier.researcheridD-7762-2012cs
dc.identifier.researcheridH-8100-2017cs
dc.identifier.researcheridG-9463-2014cs
dc.identifier.researcheridD-6800-2012cs
dc.identifier.scopus57990461800cs
dc.identifier.scopus25621760100cs
dc.identifier.scopus12039667200cs
dc.identifier.scopus55312098800cs
dc.identifier.scopus7402184758cs
dc.identifier.urihttps://hdl.handle.net/11012/249757
dc.language.isoencs
dc.publisherROYAL SOC CHEMISTRYcs
dc.relation.ispartofJournal of Analalytical Atomic Spectrometrycs
dc.relation.urihttps://pubs.rsc.org/en/content/articlelanding/2024/ja/d4ja00073kcs
dc.rightsCreative Commons Attribution-NonCommercial 4.0 Internationalcs
dc.rights.accessopenAccesscs
dc.rights.sherpahttp://www.sherpa.ac.uk/romeo/issn/0267-9477/cs
dc.rights.urihttp://creativecommons.org/licenses/by-nc/4.0/cs
dc.subjectInduced breakdown spectroscopyen
dc.subjectBiomedical Applicationsen
dc.subject1064 NMen
dc.subjectTeethen
dc.titleInvestigating the effects of laser wavelengths and other ablation parameters on the detection of biogenic elements and contaminants in hydroxyapatiteen
dc.type.driverarticleen
dc.type.statusPeer-revieweden
dc.type.versionpublishedVersionen
sync.item.dbidVAV-189905en
sync.item.dbtypeVAVen
sync.item.insts2024.12.10 14:55:41en
sync.item.modts2024.12.10 11:32:06en
thesis.grantorVysoké učení technické v Brně. Středoevropský technologický institut VUT. Pokročilé instrumentace a metody pro charakterizace materiálůcs
thesis.grantorVysoké učení technické v Brně. Středoevropský technologický institut VUT. Pokročilé biomateriálycs
thesis.grantorVysoké učení technické v Brně. Fakulta strojního inženýrství. Ústav fyzikálního inženýrstvícs
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