Dilatometric and microstructural study of particle and functionally graded composites based on hydroxyapatite and crystalline bioglass

dc.contributor.authorDrdlík, Danielcs
dc.contributor.authorDrdlíková, Katarinacs
dc.contributor.authorMaca, Karelcs
dc.coverage.issue3cs
dc.coverage.volume55cs
dc.date.accessioned2024-02-20T10:45:49Z
dc.date.available2024-02-20T10:45:49Z
dc.date.issued2023-10-23cs
dc.description.abstractHydroxyapatite (HA) and bioglass (BG) ceramics have become of prime importance in bone tissue engineering. Besides the appropriate composition, the microstructure of bone replacement plays a crucial role. In the present work, particle composites and functionally graded material (FGM) based on HA and BG prepared by electrophoretic deposition were thoroughly characterised in terms of the preparation method, sintering process, phase composition and microstructure. The sintering was monitored by high-temperature dilatometry in two directions, the sintering rates were calculated, and the overall sintering process was discussed. The SEM showed the continuous change in the microstructure of FGM with gradual interconnected porosity favourable for bio-applications. The fundamental fractographic analysis proved the crack development in FGM related to the sintering process, and the recommendations for the reduction of the crack development were given. The phase transformations during thermal treatment were analysed using X-ray diffraction analysis and deeply discussed.en
dc.formattextcs
dc.format.extent289-306cs
dc.format.mimetypeapplication/pdfcs
dc.identifier.citationScience of Sintering. 2023, vol. 55, issue 3, p. 289-306.en
dc.identifier.doi10.2298/SOS221028017Dcs
dc.identifier.issn0350-820Xcs
dc.identifier.orcid0000-0003-4545-7779cs
dc.identifier.orcid0000-0002-7535-6920cs
dc.identifier.other184960cs
dc.identifier.researcheridE-1633-2012cs
dc.identifier.researcheridD-7520-2012cs
dc.identifier.scopus51863504600cs
dc.identifier.scopus6603065815cs
dc.identifier.urihttps://hdl.handle.net/11012/245085
dc.language.isoencs
dc.relation.ispartofScience of Sinteringcs
dc.relation.urihttp://ojs.itn.sanu.ac.rs/index.php/scisint/article/view/1099cs
dc.rightsCreative Commons Attribution 4.0 Internationalcs
dc.rights.accessopenAccesscs
dc.rights.sherpahttp://www.sherpa.ac.uk/romeo/issn/0350-820X/cs
dc.rights.urihttp://creativecommons.org/licenses/by/4.0/cs
dc.subjectBioglassen
dc.subjectFunctionally graded materialen
dc.subjectHydroxyapatiteen
dc.subjectMicrostructureen
dc.subjectSinteringen
dc.titleDilatometric and microstructural study of particle and functionally graded composites based on hydroxyapatite and crystalline bioglassen
dc.type.driverarticleen
dc.type.statusPeer-revieweden
dc.type.versionpublishedVersionen
sync.item.dbidVAV-184960en
sync.item.dbtypeVAVen
sync.item.insts2024.02.20 11:45:49en
sync.item.modts2024.02.20 11:13:01en
thesis.grantorVysoké učení technické v Brně. Středoevropský technologický institut VUT. Pokročilá multifunkční keramikacs
thesis.grantorVysoké učení technické v Brně. Fakulta strojního inženýrství. ÚMVI-odbor keramiky a polymerůcs
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