Thermodynamics of Crystals Formation and Growth in a Sessile Droplet

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dc.contributor.authorZhu, Hanliangcs
dc.contributor.authorZhang, Yuecs
dc.contributor.authorLu, Haiyangcs
dc.contributor.authorFeng, Jianguocs
dc.contributor.authorYan, Qi-Longcs
dc.contributor.authorBrodský, Jancs
dc.contributor.authorGablech, Imrichcs
dc.contributor.authorNeužil, Pavelcs
dc.coverage.issue6cs
dc.coverage.volume5cs
dc.date.accessioned2025-02-03T14:41:27Z
dc.date.available2025-02-03T14:41:27Z
dc.date.issued2024-05-09cs
dc.description.abstractAccurately detecting subtle thermodynamics during crystallization and associated water evaporation processes, especially around seed formation, has been challenging. Here, we report a method to investigate the complex energy changes during these simultaneous endothermic and exothermic events. We employ an open-space microcalorimeter, coupled with optical observation using a microscope equipped with a camera for real-time monitoring. This method reveals crystal formation by observing energy changes and simultaneously visualizing the sample. The concentration influence for potassium chloride crystallization is analyzed, including energy released and the evaporation thermodynamics using isothermal microcalorimetry. We also monitor the energy dissipation during crystallization, showing an 4.2 s period for potassium chloride crystal seed formation with a released energy of 11.9 J. This method can potentially reshape strategies for controlled crystallization across diverse industrial and laboratory settings. Extending beyond potassium chloride, our findings shed light on broader crystallization dynamics, paving the way for innovations in materials and energy sciences.en
dc.formattextcs
dc.format.extent1-15cs
dc.format.mimetypeapplication/pdfcs
dc.identifier.citationCell Reports Physical Science. 2024, vol. 5, issue 6, p. 1-15.en
dc.identifier.doi10.1016/j.xcrp.2024.101971cs
dc.identifier.issn2666-3864cs
dc.identifier.orcid0000-0002-5656-3158cs
dc.identifier.orcid0000-0003-4218-1287cs
dc.identifier.other188442cs
dc.identifier.researcheridGYJ-6288-2022cs
dc.identifier.researcheridH-7835-2016cs
dc.identifier.scopus57212587388cs
dc.identifier.scopus55091127400cs
dc.identifier.urihttps://hdl.handle.net/11012/249912
dc.language.isoencs
dc.publisherCell Presscs
dc.relation.ispartofCell Reports Physical Sciencecs
dc.relation.urihttps://www.sciencedirect.com/science/article/pii/S0165993624001584cs
dc.rightsCreative Commons Attribution-NonCommercial 4.0 Internationalcs
dc.rights.accessopenAccesscs
dc.rights.sherpahttp://www.sherpa.ac.uk/romeo/issn/2666-3864/cs
dc.rights.urihttp://creativecommons.org/licenses/by-nc/4.0/cs
dc.subjectenergy dissipationen
dc.subjectmicrocalorimetryen
dc.subjectsalt crystallizationen
dc.subjectcrystal seed formationen
dc.subjectthermodynamicsen
dc.titleThermodynamics of Crystals Formation and Growth in a Sessile Dropleten
dc.type.driverarticleen
dc.type.statusPeer-revieweden
dc.type.versionpublishedVersionen
sync.item.dbidVAV-188442en
sync.item.dbtypeVAVen
sync.item.insts2025.02.03 15:41:27en
sync.item.modts2025.01.17 15:24:53en
thesis.grantorVysoké učení technické v Brně. Fakulta elektrotechniky a komunikačních technologií. Ústav mikroelektronikycs
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